Hydrochloric Acid → HCID 178455960, 화합물

HRID 1395819노트

반응식

HRID 1395819 반응식
[CH3:1][O:2][C:3](=[O:40])[C@H:4]([CH2:38][OH:39])[NH:5][C:6](=[O:37])[C@@H:7]1[CH2:11][CH2:10][CH2:9][N:8]1[C:12](=[O:36])[C@H:13]([CH2:30][C:31]1[N:35]=[CH:34][NH:33][CH:32]=1)[NH:14][C:15](=[O:29])[C@H:16]([C@H:25]([CH2:27][CH3:28])[CH3:26])[NH:17]C(OC(C)(C)C)=O.[ClH:41]>O1CCOCC1>[ClH:41].[CH3:1][O:2][C:3](=[O:40])[C@H:4]([CH2:38][OH:39])[NH:5][C:6](=[O:37])[C@@H:7]1[CH2:11][CH2:10][CH2:9][N:8]1[C:12](=[O:36])[C@H:13]([CH2:30][C:31]1[N:35]=[CH:34][NH:33][CH:32]=1)[NH:14][C:15](=[O:29])[C@H:16]([C@H:25]([CH2:27][CH3:28])[CH3:26])[NH2:17]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 178455967HCID 178455967, 화합물

생성물 1

HCID 178455960HCID 178455960, 화합물

시약·촉매·용매 1

HCID 312751,4-Dioxane용매2회

실험 절차

8.5 g of t-butoxycarbonylisoleucylhistidylprolylserine methyl ester is dissolved in 51 ml of dioxane. To this solution is added 25.5 ml of 6 N hydrochloric acid in dioxane. The reaction is allowed to stand for ten minutes and the solvent is removed under vacuum to afford isoleucylhistidylprolylserine methyl ester hydrochloride.

후처리

  1. waitto stand for ten minutes
  2. customthe solvent is removed under vacuum

출처 및 근거

ORD 기록
ord-822003db699843fabbe710af602cfa63
출처 데이터셋
uspto-grants-1980_05
특허 번호
US04204991

반응 노트

불러오는 중…