Methyl iodide → HCID 178442415, 화합물

반응식

[CH2:1]([C:7]1[N:8]=[N:9][N:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[I:18][CH3:19]>>[I-:18].[CH2:1]([C:7]1[N+:8]([CH3:19])=[N:9][N:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

참가 물질

반응물 2

HCID 6328Methyl iodide2회

HCID 67202007HCID 67202007, 화합물

생성물 1

HCID 178442415HCID 178442415, 화합물

반응 조건

온도: 40 °C

실험 절차

4-hexyl-1-phenyl-1H-1,2,3-triazole and excess iodomethane were added to a 20 mL vial. The reaction was heated at 40° C. for 3 days. The iodomethane was allowed to evaporate in the hood. The following structure of 4-hexyl-3-methyl-1-phenyl-1H-1,2,3-triazol-3-ium iodide was confirmed:

후처리

customto evaporate in the hood

출처 및 근거

ORD 기록: ord-9755083dcd4a48e19e95da602cc4fa2f
출처 데이터셋: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08906135B1

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