Hydrochloric Acid → HCID 67407911, 화합물

HRID 1401261노트

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HRID 1401261 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:20])[C:11]=3[C@@H:21]2[CH2:25][CH2:24][N:23]([CH3:26])[C@H:22]2[CH2:27][OH:28])[CH:5]=[CH:6][CH:7]=1.Cl>CO>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([C:8]2[O:9][C:10]3[C:15]([C:16](=[O:18])[CH:17]=2)=[C:14]([OH:19])[CH:13]=[C:12]([OH:20])[C:11]=3[C@@H:21]2[CH2:25][CH2:24][N:23]([CH3:26])[C@H:22]2[CH2:27][OH:28])[CH:5]=[CH:6][CH:7]=1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 66933697HCID 66933697, 화합물

생성물 1

HCID 67407911HCID 67407911, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The compound of example 33 (0.140 g, 0.349 mmol) was suspended in methanol (2 mL) and treated with ethereal HCl and the organic solvent was evaporated to afford the title compound, the hydrochloride salt.

후처리

  1. customthe organic solvent was evaporated

출처 및 근거

ORD 기록
ord-7c7420cd496e45b1aba1b56761e3cd58
출처 데이터셋
uspto-grants-2014_12
특허 번호
US08906953B2

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