Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Dibutylamino)ethanol → 1-Butanaminium, N,N-dibutyl-N-(2-hydroxyethyl)-, chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Dibutylamino)ethanol | HCID 7621 | — |
| 반응물 | Butyl Chloride | HCID 8005 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Butanaminium, N,N-dibutyl-N-(2-hydroxyethyl)-, chloride | HCID 71334730 | 100% |
반응 단계
70 mmol of 2-(dibutylamino) ethanol, 75 mmol of 1-chlorobutane, and 50 g of ethanol were mixed under N2 atmosphere, and made to react at 80 degrees C. for 8 hours under reflux condition. The ethanol and extra 1-chlorobutane were distilled away therefrom by reducing pressure to produce 70 mmol of (2-hydroxyethyl)tributylammonium chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08913931B2 |
| 출처 데이터셋 | uspto-grants-2014_12 |
| ORD ID | ord-4c9a2167d0b84e86a953d28febca755f |
| 출처 메모 | uspto-grants-2014_12 |