Ethyl 2-fluoro-4-(methylamino)-5-nitrobenzoate → 5-Amino-2-fluoro-4-methylamino-benzoic acid ethyl ester
반응식
[CH2:1]([O:3][C:4](=[O:17])[C:5]1[CH:10]=[C:9]([N+:11]([O-])=O)[C:8]([NH:14][CH3:15])=[CH:7][C:6]=1[F:16])[CH3:2]>[Ni].C1COCC1>[CH2:1]([O:3][C:4](=[O:17])[C:5]1[CH:10]=[C:9]([NH2:11])[C:8]([NH:14][CH3:15])=[CH:7][C:6]=1[F:16])[CH3:2]참가 물질
4
실험 절차
Prepared analogously to example 14b by hydrogenation of 2-fluoro-4-methylamino-5-nitro-benzoic acid ethyl ester using Raney nickel in THF.
출처 및 근거
- ORD 기록
- ord-49fcf5150b124180af714e41c9f752a6
- 출처 데이터셋
- uspto-grants-2014_12
- 특허 번호
- US08916599B2
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