Lithium Hydroxide → HCID 71093780, 화합물
반응식
C([O:3][C:4]([C:6]1[N:10]=[C:9]([C:11]2[CH:16]=[CH:15][C:14]([C:17]#[N:18])=[CH:13][C:12]=2[F:19])[O:8][N:7]=1)=[O:5])C.[Li+].[OH-]>O1CCCC1>[C:17]([C:14]1[CH:15]=[CH:16][C:11]([C:9]2[O:8][N:7]=[C:6]([C:4]([OH:5])=[O:3])[N:10]=2)=[C:12]([F:19])[CH:13]=1)#[N:18]참가 물질
4
실험 절차
The title compound is prepared from 5-(4-cyano-2-fluoro-phenyl)-[1,2,4]oxadiazole-3-carboxylic acid ethyl ester by treatment with aqueous LiOH solution in tetrahydrofuran. LC (method 15): tR=0.69 min; Mass spectrum (ESI+): m/z=234 [M+H]+.
출처 및 근거
- ORD 기록
- ord-763f4122caee4f399fd63f9b872ac1e5
- 출처 데이터셋
- uspto-grants-2014_12
- 특허 번호
- US08921398B2
반응 노트
불러오는 중…