참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 5-Fluorouracil | HCID 3385 | — |
| 반응물 | 2,3-Dihydrofuran | HCID 70934 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 1,3-Bis(tetrahydro-2-furanyl)-5-fluoro-2,4-pyrimidinedione | HCID 124956 | — |
반응 단계
In 20.8 ml of pyridine were dissolved 5.2 g (40 m mol) of 5-fluorouracil and 9.8 g (140 m mol) of 2,3-dihydrofuran. The solution was heated at about 160° C. in a closed tubular reactor under agitation for 5 hours. The resultant reaction mixture was treated similarly to Example 7 to give the above mentioned-compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04249006 |
|---|
| 출처 데이터셋 | uspto-grants-1981_02 |
|---|
| ORD ID | ord-1ea1786e9d7141798e9e1650d0b1a6f5 |
|---|
| 출처 메모 | uspto-grants-1981_02 |
|---|
