HRID1413197

反应详情

EQUATION

反应方程式

HRID 1413197 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
160 °C

PROCEDURE

实验过程

In 20.8 ml of pyridine were dissolved 5.2 g (40 m mol) of 5-fluorouracil and 9.8 g (140 m mol) of 2,3-dihydrofuran. The solution was heated at about 160° C. in a closed tubular reactor under agitation for 5 hours. The resultant reaction mixture was treated similarly to Example 7 to give the above mentioned-compound.

WORKUP

后处理

  1. customThe resultant reaction mixture
  2. additionwas treated similarly to Example 7
  3. customto give the above mentioned-compound