Phosphorus sulfide (P2S5) → HCID 13548752, 화합물
반응식
[CH3:1][C:2]1[N:3]=[C:4]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[N:5]2[C:10]=1[CH:9]=[N:8][NH:7][C:6]2=O.P12(SP3(SP(SP(S3)(S1)=S)(=S)S2)=S)=[S:19]>N1C=CC=CC=1>[CH3:1][C:2]1[N:3]=[C:4]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[N:5]2[C:10]=1[CH:9]=[N:8][NH:7][C:6]2=[S:19]참가 물질
4
반응 조건
- 온도
- 100 °C
실험 절차
To a solution of 4.5 gm. of 8-methyl-6-phenyl-imidazo-[1,5-d]-as-triazin-4(3H)-one in 100 ml. of pyridine is added 5 gm. of phosphorus pentasulfide. The reaction mixture is heated at 100° C. for 8 hours, filtered, and poured into dilute hydrochloric acid. The precipitated product is isolated by filtration, washed with water, and dried.
후처리
- filtrationfiltered
- additionpoured into dilute hydrochloric acid
- customThe precipitated product is isolated by filtration
- washwashed with water
- customdried
출처 및 근거
- ORD 기록
- ord-89b394a74f8f45bebf236b02e3b6ed7d
- 출처 데이터셋
- uspto-grants-1981_02
- 특허 번호
- USRE030511
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