1-Nitro-4-(3-phenylpropoxy)benzene → Aniline, p-(3-phenylpropoxy)-

HRID 1415348노트

반응식

HRID 1415348 반응식
[C:1]1([CH2:7][CH2:8][CH2:9][O:10][C:11]2[CH:16]=[CH:15][C:14]([N+:17]([O-])=O)=[CH:13][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>CO.[Ni].[H][H]>[C:1]1([CH2:7][CH2:8][CH2:9][O:10][C:11]2[CH:12]=[CH:13][C:14]([NH2:17])=[CH:15][CH:16]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

5

반응물 1

HCID 214818451-Nitro-4-(3-phenylpropoxy)benzene

생성물 1

HCID 42154Aniline, p-(3-phenylpropoxy)-

시약·촉매·용매 3

HCID 935Nickel촉매HCID 887Methanol용매HCID 178418361HCID 178418361, 화합물용매

실험 절차

99 g of 4-(3'-phenyl-propoxy)-nitrobenzene is dissolved in 2000 ml of methanol and hydrogenated with Raney nickel until the absorption of hydrogen is completed. The catalyst is filtered off and the filtrate is concentrated by evaporation to obtain, as a crystalline residue, 4-(3'-phenylpropoxy)-aniline having a melting point of 55°- 57°. -

후처리

  1. filtrationThe catalyst is filtered off
  2. concentrationthe filtrate is concentrated by evaporation

출처 및 근거

ORD 기록
ord-b76eb5365a4e442faeb86e2e4339cc8a
출처 데이터셋
uspto-grants-1977_01
특허 번호
US04004907

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