Hydrochloric Acid → 5-Benzyloxytryptamine hydrochloride

HRID 1415508노트

반응식

HRID 1415508 반응식
C(OCC)(=O)C.[ClH:7].[CH2:8]([O:15][C:16]1[CH:27]=[C:26]2[C:19]([NH:20][CH:21]=[C:22]2[CH2:23][CH2:24][NH2:25])=[CH:18][CH:17]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>C(O)(C)C>[ClH:7].[CH2:8]([O:15][C:16]1[CH:27]=[C:26]2[C:19]([NH:20][CH:21]=[C:22]2[CH2:23][CH2:24][NH2:25])=[CH:18][CH:17]=1)[C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 8857Ethyl AcetateHCID 895765-(Benzyloxy)tryptamine

생성물 1

HCID 28287855-Benzyloxytryptamine hydrochloride

시약·촉매·용매 1

HCID 3776Isopropanol용매

실험 절차

An ethyl acetate solution saturated with hydrochloric acid was added to a solution of 10 g of 5-benzyloxy-tryptamine in 200 ml of isopropanol until the pH was 1-2 and the mixture was vacuum filtered. The crystals were washed with ethyl acetate and dried under reduced pressure to obtain 11.3 g of 5-benzyloxy-tryptamine hydrochloride melting at 250° C.

후처리

  1. filtrationfiltered
  2. washThe crystals were washed with ethyl acetate
  3. customdried under reduced pressure

출처 및 근거

ORD 기록
ord-1c1a01720dc44e5eb030897af143d39e
출처 데이터셋
uspto-grants-1977_01
특허 번호
US04005206

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