Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethylenediamine → N-[2-Hydroxy-2-(4-methoxyphenyl)ethyl]-ethylenediamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethylenediamine | HCID 3301 | — |
| 반응물 | 2-(4-Methoxyphenyl)oxirane | HCID 98048 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-[2-Hydroxy-2-(4-methoxyphenyl)ethyl]-ethylenediamine | HCID 21482929 | — |
반응 단계
N-[2-Hydroxy-2-(4-methoxyphenyl)ethyl]-ethylenediamine is prepared by reacting 2-(4-methoxyphenyl)oxirane (37.5 g.) dissolved in methanol (52 cc.) with ethylenediamine (30 cc.) dissolved in a mixture of methanol (52 cc.) and water (20 cc.). On distillation under reduced pressure, a product (22.3 g.), b.p. 165°-169° C./0.2 mm.Hg, is obtained, which crystallises on cooling and melts at 68° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04005212 |
| 출처 데이터셋 | uspto-grants-1977_01 |
| ORD ID | ord-8e3fe7b98a9543bcb984cc75cb887cb4 |
| 출처 메모 | uspto-grants-1977_01 |