Water → HCID 11311579, 화합물

HRID 1420768노트

반응식

HRID 1420768 반응식
[Na].[C:2]([O:6][CH3:7])(=[O:5])[CH2:3][SH:4].C1(S(O[CH:18]=[C:19]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=2[O:28][CH3:29])[C:20]#[N:21])(=O)=O)C=CC=CC=1.O>CO>[NH2:21][C:20]1[C:19]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=2[O:28][CH3:29])=[CH:18][S:4][C:3]=1[C:2]([O:6][CH3:7])=[O:5]

참가 물질

6

반응물 4

HCID 962WaterHCID 16907Methyl ThioglycolateHCID 5360545SodiumHCID 57066737alpha-(Phenylsulphonyloxymethylidene)-2-methoxyphenylacetonitrile

생성물 1

HCID 11311579HCID 11311579, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

11 mmol of sodium are dissolved in 100 ml of methanol. After cooling the reaction mixture using an ice bath, 4.5 mmol of methyl thioglycolate and then 3.7 mmol of the compound obtained in Step B are added. After 2 hours' reaction, 100 ml of water are added, bringing about the formation of a precipitate, which is filtered off and then dried, allowing the to expected product to be isolated.

후처리

  1. temperatureAfter cooling the reaction mixture
  2. additionare added
  3. filtrationis filtered off
  4. customdried
  5. customto be isolated

출처 및 근거

ORD 기록
ord-6bb6e1869add43ff9cb4880ebd322549
출처 데이터셋
uspto-grants-2000_06
특허 번호
US06071945

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