Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 3-(Benzyloxy)-4-methoxybenzyl alcohol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 3-Benzyloxy-4-methoxybenzaldehyde | HCID 80671 | — |
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 3-(Benzyloxy)-4-methoxybenzyl alcohol | HCID 74622 | — |
반응 단계
A solution of 0.35 mol of the compound obtained in Step 1 in 400 ml of methanol and 1.5 equivalents of sodium borohydride is stirred for 6 hours at ambient temperature and then 500 ml of acidified water are slowly added. The precipitate obtained is taken up in ether; the organic phase is subsequently extracted, dried, filtered and then evaporated off under reduced pressure, allowing the expected product to be isolated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06071945 |
| 출처 데이터셋 | uspto-grants-2000_06 |
| ORD ID | ord-fc144128b9d74547bc6aca0d6074e7de |
| 출처 메모 | uspto-grants-2000_06 |