3-Phenylprop-2-Enal → Cinnamyl Alcohol
반응식
[CH:1](=[O:10])[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.CCCCCCCCCCCC>C(O)(C)C>[CH:7]1[CH:6]=[CH:5][C:4](/[CH:3]=[CH:2]/[CH2:1][OH:10])=[CH:9][CH:8]=1참가 물질
4
실험 절차
In a three-necked flask provided with reflux condenser and magnetic stirrer, 0.5 g (3.8 mmol) of cinnamaldehyde (trans-3-phenyl-2-propanol) and 12 g of isopropyl alcohol (for a starting material/catalyst ratio=1:1) or 1.5 g (11.3 mmol) of cinnamaldehyde and 36 g of isopropyl alcohol (starting material/catalyst=3:1) were refluxed under argon with 0.5 g of catalyst and 1.5 g of dodecane (as GC standard). After the end of the reaction time, the reaction mixture was analyzed by gas chromatography and the yield was determined. The results are summarized in Table 2 below:
후처리
- customIn a three-necked flask provided
- temperaturewith reflux condenser and magnetic stirrer
출처 및 근거
- ORD 기록
- ord-b3fef801a55e43e4a4d8415454df9456
- 출처 데이터셋
- uspto-grants-2000_06
- 특허 번호
- US06075145
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