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Thiourea → S-(4-(4-chlorobenzoyl)benzyl)thiouronium bromide

HRID 1421546
노트
인쇄 미리보기

반응식

HRID 1421546 반응식
[Br:1][CH2:2][C:3]1[CH:17]=[CH:16][C:6]([C:7]([C:9]2[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][CH:10]=2)=[O:8])=[CH:5][CH:4]=1.[NH2:18][C:19]([NH2:21])=[S:20]>CC(C)=O>[Br-:1].[Cl:15][C:12]1[CH:13]=[CH:14][C:9]([C:7]([C:6]2[CH:16]=[CH:17][C:3]([CH2:2][S:20][C:19]([NH2:21])=[NH2+:18])=[CH:4][CH:5]=2)=[O:8])=[CH:10][CH:11]=1
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참가 물질

4

반응물 2

HCID 2723790ThioureaHCID 98396514-(4-Chlorobenzoyl)benzyl bromide

생성물 1

HCID 18779877S-(4-(4-chlorobenzoyl)benzyl)thiouronium bromide수율 85.4%

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

An acetone solution (500 ml) of 4-bromomethyl-4'-chlorobenzophenone (31 g) and thiourea (10 g) was heated for 30 minutes with refluxing. The precipitated crystals were then collected by filtration and washed with acetone to obtain S-(4-(4-chlorobenzoyl)benzyl)thiouronium bromide (33 g).

후처리

  1. temperaturewith refluxing
  2. filtrationThe precipitated crystals were then collected by filtration
  3. washwashed with acetone

출처 및 근거

ORD 기록
ord-856fc1cebc144e7eb88891a8c8c5cbd4
출처 데이터셋
uspto-grants-2000_06
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06077866

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