5-Chloro-2-ethoxybenzoic acid → HCID 85827033, 화합물

HRID 1435732

반응식

HRID 1435732 반응식
[Cl:1][C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([C:9]2[CH:14]=[C:13]([Cl:15])[CH:12]=[CH:11][C:10]=2C)[N:3]=1.ClC1C=CC(OCC)=[C:22](C=1)[C:23](O)=[O:24]>>[Cl:8][C:6]1[N:7]=[C:2]([Cl:1])[N:3]=[C:4]([C:9]2[CH:14]=[C:13]([Cl:15])[CH:12]=[CH:11][C:10]=2[O:24][CH2:23][CH3:22])[N:5]=1

참가 물질

3

반응물 2

HCID 50985705-Chloro-2-ethoxybenzoic acidHCID 858270322,4-Dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine

생성물 1

HCID 85827033HCID 85827033, 화합물수율 31%

실험 절차

Using the method described for the synthesis of 2,4-dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine, 5-chloro-2-ethoxybenzoic acid afforded 2,4-dichloro-6-(5-chloro-2-ethoxy-phenyl)-[1,3,5]triazine (9.5 g, 31% yield). 1H NMR (DMSO-d6) 7.62-7.86 (m, 2H), 7.20-7.31 (m, 1H), 4.20 (m, 2H), 1.37 (m, 3H).

출처 및 근거

ORD 기록
ord-0d9ef5c6beb446389066bdf434832052
출처 데이터셋
uspto-grants-2009_11
특허 번호
US07618968B2

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