2,5-Dichlorobenzoic acid → 2,4-Dichloro-6-(2,5-dichlorophenyl)-1,3,5-triazine

HRID 1435733

반응식

HRID 1435733 반응식
[Cl:1][C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([C:9]2[CH:14]=[C:13]([Cl:15])[CH:12]=[CH:11][C:10]=2C)[N:3]=1.[Cl:17]C1C=CC(Cl)=CC=1C(O)=O>>[Cl:1][C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([C:9]2[CH:14]=[C:13]([Cl:15])[CH:12]=[CH:11][C:10]=2[Cl:17])[N:3]=1

참가 물질

3

반응물 2

HCID 57842,5-Dichlorobenzoic acidHCID 858270322,4-Dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine

생성물 1

HCID 204803862,4-Dichloro-6-(2,5-dichlorophenyl)-1,3,5-triazine수율 14%

실험 절차

Using the method described for the synthesis of 2,4-dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine, 2,5-dichlorobenzoic acid afforded 2,4-dichloro-6-(2,5-dichloro-phenyl)-[1,3,5]triazine (2.2 g, 14% yield). 1H NMR (DMSO-d6) 8.10 (s, 1H), 7.50 (m, 2H).

출처 및 근거

ORD 기록
ord-0e171e5dcf604b95ac974cec699bd988
출처 데이터셋
uspto-grants-2009_11
특허 번호
US07618968B2

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