1,3-Benzodioxole-5-carbonyl chloride → 1-Amino-3-[(1,1-dimethylethyl)(phenylmethyl)amino]propan-2-OL

HRID 1439428

반응식

HRID 1439428 반응식
Cl.C1OC2C=CC(C([NH:9][CH2:10][CH:11]([OH:25])[CH2:12][N:13]([C:21]([CH3:24])([CH3:23])[CH3:22])[CH2:14][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=O)=CC=2O1.C1OC2C=CC(C(Cl)=O)=CC=2O1>>[NH2:9][CH2:10][CH:11]([OH:25])[CH2:12][N:13]([C:21]([CH3:23])([CH3:22])[CH3:24])[CH2:14][C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1

참가 물질

3

반응물 2

HCID 27347491,3-Benzodioxole-5-carbonyl chlorideHCID 1317109511-(3,4-methylenedioxy benzamido)-3-(N-benzyl tert-butylamino)-2-propanol hydrochloride

생성물 1

HCID 30165241-Amino-3-[(1,1-dimethylethyl)(phenylmethyl)amino]propan-2-OL수율 80%

실험 절차

1-(3,4-methylenedioxy benzamido)-3-(N-benzyl tert-butylamino)-2- propanol hydrochloride, starting from 6.3 g (0.034 mole) of 3,4-methylenedioxy benzoyl chloride and 8 g (0.034 mole) of 1-amino-3-(N-benzyl tert-butylamino)-2- propanol (yield 80 %).

출처 및 근거

ORD 기록
ord-a4eacd56c26c4074825c045d053fe73e
출처 데이터셋
uspto-grants-1977_11
특허 번호
US04059621

연결된 노트

불러오는 중…