Benzaldehyde → N-Benzylidene(piperidin-4-yl)methanamine

HRID 1444096

반응식

HRID 1444096 반응식
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH2:9][CH2:10][CH:11]1[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]1>C1(C)C=CC=CC=1>[NH:14]1[CH2:15][CH2:16][CH:11]([CH2:10][N:9]=[CH:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH2:12][CH2:13]1

참가 물질

4

반응물 2

HCID 240BenzaldehydeHCID 235274-(Aminomethyl)piperidine

생성물 1

HCID 11820173N-Benzylidene(piperidin-4-yl)methanamine

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Benzaldehyde (4.6 g; 0.044 mol) was added dropwise to a solution of 4-aminomethylpiperidine (5.0 g; 0.044 mol) in toluene (20 ml). The solution thus obtained was stirred for 3 h at room temperature. Then the solvent was removed by evaporation at reduced pressure and the residue was taken up twice with toluene to give the desired product that was used as such without further purification.

후처리

  1. customThe solution thus obtained
  2. customThen the solvent was removed by evaporation at reduced pressure

출처 및 근거

ORD 기록
ord-5924d5348ad944b5b28619e072e9943f
출처 데이터셋
uspto-grants-2010_02
특허 번호
US07662836B2

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