Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → N-Benzylidene(piperidin-4-yl)methanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | 4-(Aminomethyl)piperidine | HCID 23527 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-Benzylidene(piperidin-4-yl)methanamine | HCID 11820173 | — |
반응 단계
Benzaldehyde (4.6 g; 0.044 mol) was added dropwise to a solution of 4-aminomethylpiperidine (5.0 g; 0.044 mol) in toluene (20 ml). The solution thus obtained was stirred for 3 h at room temperature. Then the solvent was removed by evaporation at reduced pressure and the residue was taken up twice with toluene to give the desired product that was used as such without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07662836B2 |
| 출처 데이터셋 | uspto-grants-2010_02 |
| ORD ID | ord-5924d5348ad944b5b28619e072e9943f |
| 출처 메모 | uspto-grants-2010_02 |