Hydrochloric Acid → HCID 67143055, 화합물

HRID 1445126노트

반응식

HRID 1445126 반응식
[F:1][C:2]1[CH:22]=[CH:21][C:5]([CH2:6][NH:7][C:8]2[N:9]=[C:10]([C:19]#[N:20])[CH:11]=[C:12]3[C:16]([CH3:17])=[C:15]([CH3:18])[NH:14][C:13]=23)=[CH:4][CH:3]=1.[ClH:23]>C(OCC)(=O)C>[ClH:23].[F:1][C:2]1[CH:22]=[CH:21][C:5]([CH2:6][NH:7][C:8]2[N:9]=[C:10]([C:19]#[N:20])[CH:11]=[C:12]3[C:16]([CH3:17])=[C:15]([CH3:18])[NH:14][C:13]=23)=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 67142016HCID 67142016, 화합물

생성물 1

HCID 67143055HCID 67143055, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

A solution of 7-(4-fluorobenzylamino)-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-5-carbonitrile prepared in Step 1 in ethyl acetate was saturated with hydrochloric acid gas and then filtered to give 3.2 mg of the titled compound as a white solid.

후처리

  1. filtrationfiltered

출처 및 근거

ORD 기록
ord-d7cad497ab9e41a4bce7ca1b5b2aeacd
출처 데이터셋
uspto-grants-2010_02
특허 번호
US07662832B2

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