Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5,6-Dichloro-1H-benzimidazole → HCID 178478377, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5,6-Dichloro-1H-benzimidazole | HCID 331775 | — |
| 반응물 | 2,6-Dichloropurine | HCID 5324412 | — |
| 용매 | 1-Butanol | HCID 263 | — |
| 생성물 | HCID 178478377 | HCID 178478377 | 53.8% |
반응 단계
567 mg of 2,6-dichloropurine, 6 ml of butanol and 617 mg of 5,6-dichlorobenzimidazole are mixed and brought to a temperature of 100° C. for approximately 24 hours. The mixture is allowed to return to ambient temperature. Partial drying, washing with isopropanol and drying under vacuum at 50° C. are carried out, and 548 mg of expected product are obtained, in the form of gray/black-colored crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07476670B2 |
| 출처 데이터셋 | uspto-grants-2009_01 |
| ORD ID | ord-76e0f40d11ff49809c50455260d74855 |
| 출처 메모 | uspto-grants-2009_01 |