Dimethylformamide dimethyl acetal → 51519-09-6

HRID 1454800노트

반응식

HRID 1454800 반응식
[NH2:1][C:2]1[CH:7]=[N:6][CH:5]=[CH:4][N:3]=1.CO[CH:10](OC)[N:11]([CH3:13])[CH3:12]>>[CH3:10][N:11]([CH3:13])[CH:12]=[N:1][C:2]1[CH:7]=[N:6][CH:5]=[CH:4][N:3]=1

참가 물질

3

반응물 2

HCID 78373Dimethylformamide dimethyl acetalHCID 78747Aminopyrazine

생성물 1

HCID 1222947551519-09-6

실험 절차

A solution of 2-aminopyrazine (16.45 g) in dimethylformamide dimethylacetal (22.4 g) was refluxed at 85° C. for 3 h, evaporated under reduced pressure, and used in the next step without further purification.

후처리

  1. customevaporated under reduced pressure
  2. customused in the next step without further purification

출처 및 근거

ORD 기록
ord-f0e41c090fba493da97c1f7fcb804e13
출처 데이터셋
uspto-grants-2009_01
특허 번호
US07482336B2

반응 노트

불러오는 중…