Water → 2-Methoxy-5-tetrazol-1-yl-benzaldehyde
반응식
[OH:1][C:2]1[CH:9]=[CH:8][C:7]([N:10]2[CH:14]=[N:13][N:12]=[N:11]2)=[CH:6][C:3]=1[CH:4]=[O:5].[C:15](=O)([O-])[O-].[K+].[K+].IC.O>CN(C)C=O>[CH3:15][O:1][C:2]1[CH:9]=[CH:8][C:7]([N:10]2[CH:14]=[N:13][N:12]=[N:11]2)=[CH:6][C:3]=1[CH:4]=[O:5]참가 물질
6
실험 절차
To a solution of 2-hydroxy-5-tetrazol-1-yl-benzaldehyde (2.63 mmol) in dimethylformamide (5 ml) was added potassium carbonate (3.95 mmol) and iodomethane (3.95 mmol) and the mixture was stirred under nitrogen atmosphere for 2 h. The mixture was poured into water (100 ml) and the white solid formed filtered to afford the title compound in a 67% yield.
후처리
- customthe white solid formed
- filtrationfiltered
출처 및 근거
- ORD 기록
- ord-b5e9d024b04a4956af7e7f333ec2180e
- 출처 데이터셋
- uspto-grants-1998_12
- 특허 번호
- US05843966
반응 노트
불러오는 중…