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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Sodium Bicarbonate → HCID 22106607, 화합물

HRID 1456312
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HRID 1456312 반응식
O1CCOC1[N:6]1[N:10]=[C:9]([S:11]([CH3:14])(=[O:13])=[O:12])[N:8]([C:15]2[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=2)[NH:7]1.[C:23](=O)(O)[O-:24].[Na+]>O1CCCC1.Cl.[Cl-].[Na+].O>[CH3:14][S:11]([C:9]1[N:8]([C:15]2[CH:16]=[CH:17][C:18]([O:21][CH3:22])=[C:19]([CH:20]=2)[CH:23]=[O:24])[N:7]=[N:6][N:10]=1)(=[O:12])=[O:13]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 2

HCID 516892Sodium BicarbonateHCID 867533893-[1,3]Dioxolan-2-yl(4-methoxy-phenyl)-5-methanesulfonyl-1H-tetrazole

생성물 1

HCID 22106607HCID 22106607, 화합물

시약·촉매·용매 3

HCID 313Hydrochloric Acid용매HCID 8028Tetrahydrofuran용매HCID 57417360Sodium chloride; water용매
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실험 절차

1-(3-[1,3]Dioxolan-2-yl(4-methoxy-phenyl)-5-methanesulfonyl-1H-tetrazole (800 mg) in tetrahydrofuran (13 ml) and hydrochloric acid (2N, 7.5 ml) was stirred at room temperature for 1.5 h. The solution was basified with sodium bicarbonate solution (8%), saturated with brine (50 ml), extracted with ether (3×50 ml), dried (Na2SO4) and evaporated to give the title compound as an orange solid (307 mg).

후처리

  1. extractionextracted with ether (3×50 ml)
  2. dry with materialdried (Na2SO4)
  3. customevaporated

출처 및 근거

ORD 기록
ord-5f0af16ecc464ebd851668131fc7ff89
출처 데이터셋
uspto-grants-1998_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05843966

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