HCID 22097108, 화합물 → HCID 22097099, 화합물
반응식
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N+:13]([O-])=O)=[C:6]([NH:8][CH2:9][C:10]([OH:12])=[O:11])[CH:7]=1>C(O)C.[Ni]>[NH2:13][C:5]1[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][C:6]=1[NH:8][CH2:9][C:10]([OH:12])=[O:11]참가 물질
4
실험 절차
19.5 g (84.6 mmol) of N-(5-chloro-2-nitrophenyl)glycine were dissolved in 250 ml of ethanol and, after addition of 5 g of Raney nickel, hydrogenated under 1 bar at 45°-50° C. The mixture was then filtered, and the filtrate was evaporated under reduced pressure to yield 15.6 g (93%) of the product.
후처리
- customat 45°-50° C
- filtrationThe mixture was then filtered
- customthe filtrate was evaporated under reduced pressure
출처 및 근거
- ORD 기록
- ord-bc4a9ad543d7438a99cf7a56535473cf
- 출처 데이터셋
- uspto-grants-1998_12
- 특허 번호
- US05852017
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