Dimethylamine → Thiram

HRID 1462240

반응식

HRID 1462240 반응식
[CH3:1][NH:2][CH3:3].[C:4](=[S:6])=[S:5]>>[CH3:1][N:2]([CH3:4])[C:3](=[S:6])[S:5][S:5][C:4](=[S:6])[N:2]([CH3:3])[CH3:1]

참가 물질

3

반응물 2

HCID 674DimethylamineHCID 6348Carbon Disulfide2회

생성물 1

HCID 5455Thiram

실험 절차

The work was carried out as in Example 3, but now the rate of addition of carbon disulfide corresponded to the rate at which dimethylamine was released during the reaction. No further carbon disulfide was added after 46 minutes and the reaction had ended after 49 minutes. This method yielded a total of 35.85 g of tetramethyl thiuram disulfide, corresponding to 99.6% of theoretical.

후처리

  1. customwas released during the reaction

출처 및 근거

ORD 기록
ord-0574f614f5e04347bb14d3948a907c4e
출처 데이터셋
uspto-grants-1984_07
특허 번호
US04459424

연결된 노트

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