Methylhydrazine → HCID 13320508, 화합물

HRID 1462351노트

반응식

HRID 1462351 반응식
[CH3:1][NH:2][NH2:3].CO[C:6]1[N:11]=[CH:10][N:9]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:8](=[O:18])[N:7]=1>C(O)C>[CH3:1][NH:2][NH:3][C:6]1[N:11]=[CH:10][N:9]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:8](=[O:18])[N:7]=1

참가 물질

4

반응물 2

HCID 6061MethylhydrazineHCID 130540494-Methoxy-1-phenyl-1,3,5-triazin-2(1H)-one

생성물 1

HCID 13320508HCID 13320508, 화합물수율 63.1%

시약·촉매·용매 1

HCID 702Ethanol용매2회

실험 절차

2.4 ml of methylhydrazine dissolved in 10 ml of absolute ethanol are added to a suspension of 4-methoxy-1-phenyl-1,2-dihydro-1,3,5-triazin-2-one (4.60 g) in 100 ml of absolute ethanol and stirred for one hour. The solid product is filtered, washed with ether and dried to give 3.10 g (63.1%) of 4-methylhydrazino-1-phenyl-s-triazin-2-one, m.p. 219° C.

후처리

  1. filtrationThe solid product is filtered
  2. washwashed with ether
  3. customdried

출처 및 근거

ORD 기록
ord-a67cf2b1f5654ac0b56e3ff8ceb438fa
출처 데이터셋
uspto-grants-1984_07
특허 번호
US04460585

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