M-Cresol → HCID 54089089, 화합물

반응식

[CH3:1][C:2]1[CH:3]=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1.[Cl:9][C:10](Cl)=[CH:11][C:12]([CH3:15])([CH3:14])[CH3:13]>>[Cl:9][CH:10]=[C:11]([O:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([CH3:1])[CH:3]=1)[C:12]([CH3:15])([CH3:14])[CH3:13]

참가 물질

반응물 2

HCID 342M-Cresol

HCID 112865761,1-Dichloro-3,3-dimethyl-1-butene

생성물 1

HCID 54089089HCID 54089089, 화합물수율 87.2%

실험 절차

Analogously to Example A6(a), 0.2 mol of 3-methylphenol and 0.1 mol of 1,1-dichloro-3,3-dimethyl-1-butene are reacted to give 19.6 g of 1-chloro-3,3-dimethyl-2-(3'-methylphenoxy)-1-butene of boiling point 95°-100° C./0.7 mm Hg. The yield is 87% of theory.

출처 및 근거

ORD 기록: ord-6ac5b276d5eb4beaa29922d781c7648c
출처 데이터셋: uspto-grants-1984_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04460793

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