Methyl iodide → HCID 178503972, 화합물

HRID 1464034노트

반응식

HRID 1464034 반응식
[C:1]1([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[NH:7][C:8]([NH2:10])=[S:9].[CH3:17][I:18]>CC(C)=O>[IH:18].[C:1]1([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[NH:7][C:8](=[NH:10])[S:9][CH3:17]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 1471602N-(1,1'-Biphenyl)-2-ylthiourea

생성물 1

HCID 178503972HCID 178503972, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

반응 조건

온도
55 °C

실험 절차

A mixture of N-(2-biphenylyl)thiourea (9.6 g), methyl iodide (2.9 ml) and acetone (100 ml) was heated at 55° C. for 3 hours to yield 1-(2-biphenylyl)-2-methyl-2-thiopseudourea hydriodide.

출처 및 근거

ORD 기록
ord-d39d322ee3714dfa836cf29a314b031e
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05302720

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