Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
M-Cresol → HCID 178484374, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | M-Cresol | HCID 342 | — |
| 반응물 | Dimethylcyanamide | HCID 15112 | — |
| 반응물 | 5-Fluoro-[1,1'-biphenyl]-2-amine hydrochloride | HCID 19089218 | — |
| 생성물 | HCID 178484374 | HCID 178484374 | — |
반응 단계
A mixture of 2-amino-5-fluorobiphenyl hydrochloride (3.6 g), N,N-dimethylcyanamide (1.68 g) and m-cresol (25 ml) was heated at 90°-95° C. for 8 hours to give N-(5-fluoro-2-biphenylyl)-N',N'-dimethylguanidine (m.p. 160°-161° C.) which was recrystallised from hexane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05302720 |
| 출처 데이터셋 | uspto-grants-1994_04 |
| ORD ID | ord-20fb8c4e79754dc3a355821d79cc8c76 |
| 출처 메모 | uspto-grants-1994_04 |