Dimethylcyanamide → HCID 178424492, 화합물

HRID 1464058노트

반응식

HRID 1464058 반응식
Cl.[NH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([CH3:15])[CH:10]=1.[CH3:16][N:17]([CH3:20])[C:18]#[N:19]>C1C(O)=CC=CC=1C>[CH3:16][N:17]([CH3:20])[C:18]([NH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([CH3:15])[CH:10]=1)=[NH:19]

참가 물질

4

반응물 2

HCID 15112DimethylcyanamideHCID 27598232-Amino-3'-methylbiphenyl hydrochloride

생성물 1

HCID 178424492HCID 178424492, 화합물

시약·촉매·용매 1

HCID 342M-Cresol용매

반응 조건

온도
100 °C

실험 절차

A mixture of 2-amino-3'-methylbiphenyl hydrochloride (1 g), N,N-dimethylcyanamide (0.67 ml) in m-cresol (1 ml) was heated at 100° C. for 3 hours to give N,N-dimethyl-N'-(3'-methyl-2-biphenylyl)guanidine (m.p. 116° C.) which was crystallised from hexane.

출처 및 근거

ORD 기록
ord-edad7aa982244479928e2ba708279ed6
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05302720

반응 노트

불러오는 중…