Potassium Hydroxide → 4-Methylthio-2-biphenylylcyanamide
반응식
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[C:5]([NH:15][C:16]([NH2:18])=S)[CH:4]=1.[OH-].[K+].O.O.O.C([O-])(=O)C.[Pb+2].C([O-])(=O)C>O>[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[C:5]([NH:15][C:16]#[N:18])[CH:4]=1참가 물질
5
실험 절차
A mixture of N-(4-methylthio-2-biphenylyl)thiourea (9.6 g), potassium hydroxide (8.5 g), lead acetate trihydrate (12.5 g) and water (165 ml) was heated at 90°-95° C. for 30 minutes to give 4-methylthio-2-biphenylylcyanamide.
후처리
- temperaturewas heated at 90°-95° C. for 30 minutes
출처 및 근거
- ORD 기록
- ord-8912914b9c024cf7b1e2f4aef4b2905a
- 출처 데이터셋
- uspto-grants-1994_04
- 특허 번호
- US05302720
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