Vinyl chloroformate → HCID 59601719, 화합물

HRID 1464861노트

반응식

HRID 1464861 반응식
[CH3:1][O:2][NH:3][C:4](=[O:7])[CH:5]=[CH2:6].[CH:8]([O:10][C:11](Cl)=[O:12])=[CH2:9]>>[CH:8]([O:10][C:11](=[O:12])[N:3]([O:2][CH3:1])[C:4](=[O:7])[CH:5]=[CH2:6])=[CH2:9]

참가 물질

3

반응물 2

HCID 78808Vinyl chloroformateHCID 13531445N-Methoxyprop-2-enamide

생성물 1

HCID 59601719HCID 59601719, 화합물

실험 절차

The synthesis was carried out analogously to synthesis example 8 using N-methoxy-acrylamide and chloroformic acid vinyl ester. Purification by column chromatography on silica gel (PE:EE=9:1) yielded 1.6 g (91% of th.) of the title compound as a colorless liquid.

후처리

  1. customPurification by column chromatography on silica gel (PE:EE=9:1)

출처 및 근거

ORD 기록
ord-5457b3292eac4bc197a3beacfcc105ba
출처 데이터셋
uspto-grants-2015_04
특허 번호
US08999323B2

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