Butyryl chloride → N-(1-hydroxy-2-methylpropan-2-yl)butyramide

반응식

[NH2:1][C:2]([CH3:6])([CH3:5])[CH2:3][OH:4].[C:7](Cl)(=[O:11])[CH2:8][CH2:9][CH3:10]>>[OH:4][CH2:3][C:2]([NH:1][C:7](=[O:11])[CH2:8][CH2:9][CH3:10])([CH3:6])[CH3:5]

참가 물질

반응물 2

HCID 8855Butyryl chloride

HCID 118072-Amino-2-methyl-1-propanol

생성물 1

HCID 12497727N-(1-hydroxy-2-methylpropan-2-yl)butyramide수율 32%

실험 절차

Prepared according to the literature (Boyd, R. N.; Hansen, R. H. J. Am. Chem. Soc. 1953, 75, 5896) from 2-amino-2-methylpropan-1-ol and butyryl chloride in 32% yield. MS 160 (MH+).

후처리

customPrepared

출처 및 근거

ORD 기록: ord-d7d9a586ed9446a781c1974424100ff2
출처 데이터셋: uspto-grants-2015_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09000054B2

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