Hydrochloric Acid → 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide hydrochloride

HRID 1476705

반응식

HRID 1476705 반응식
[NH2:1][C:2]1[CH:18]=[CH:17][CH:16]=[C:15]([S:19][C:20]2[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[CH:22][CH:21]=2)[C:3]=1[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14])=[O:5].[ClH:29]>CC(=O)OCC>[ClH:29].[NH2:1][C:2]1[CH:18]=[CH:17][CH:16]=[C:15]([S:19][C:20]2[CH:21]=[CH:22][C:23]([N+:26]([O-:28])=[O:27])=[CH:24][CH:25]=2)[C:3]=1[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14])=[O:5]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 718115872-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide

생성물 1

HCID 1183869692-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide hydrochloride수율 94.2%

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide dissolved in EA, stirred at room temperature, while HCl is inlet till occurred to white solid. The reaction mixture was filtered to get White solid; 94.2% yield;

후처리

  1. filtrationThe reaction mixture was filtered
  2. customto get White solid

출처 및 근거

ORD 기록
ord-81815eb3c1d54bb1b2ab89da27304eb8
출처 데이터셋
uspto-grants-2016_08
특허 번호
US09402819B2

연결된 노트

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