Sulfuric Acid → 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate

HRID 1476706

반응식

HRID 1476706 반응식
[NH2:1][C:2]1[CH:18]=[CH:17][CH:16]=[C:15]([S:19][C:20]2[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[CH:22][CH:21]=2)[C:3]=1[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14])=[O:5].[OH:29][S:30]([OH:33])(=[O:32])=[O:31]>CC(=O)OCC>[S:30]([OH:33])([OH:32])(=[O:31])=[O:29].[NH2:1][C:2]1[CH:18]=[CH:17][CH:16]=[C:15]([S:19][C:20]2[CH:21]=[CH:22][C:23]([N+:26]([O-:28])=[O:27])=[CH:24][CH:25]=2)[C:3]=1[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14])=[O:5]

참가 물질

4

반응물 2

HCID 1118Sulfuric AcidHCID 718115872-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide

생성물 1

HCID 1183870042-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate수율 72%

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide dissolved in EA, stirred at room temperature, while dropped H2SO4 into mixture till occurred to white solid. The reaction mixture was filtered to get White solid; 72% yield;

후처리

  1. filtrationThe reaction mixture was filtered
  2. customto get White solid

출처 및 근거

ORD 기록
ord-46c5fcb07c94481a8e8f0d3a8d9e85a9
출처 데이터셋
uspto-grants-2016_08
특허 번호
US09402819B2

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