Ethyl butyl ether → 2-(2-Butoxyethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

HRID 1490987

반응식

HRID 1490987 반응식
CCCCOCC>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CCCCOCCB1OC(C)(C)C(C)(C)O1

참가 물질

6

반응물 1

HCID 12355Ethyl butyl ether

생성물 1

HCID 860185652-(2-Butoxyethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane수율 51%

시약·촉매·용매 4

HCID 2733548Bis(pinacolato)diborane시약HCID 49133562-Methyl-1,10-phenanthroline시약HCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridium촉매HCID 9266Cyclooctane용매

반응 조건

온도
100 °C

출처 및 근거

ORD 기록
ord-647d3582d5f54beaab805edca89db85b
출처 데이터셋
Borylation dataset from Roche

연결된 노트

불러오는 중…