Hydrochloric Acid → 1H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

HRID 1491655노트

반응식

HRID 1491655 반응식
[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][N:2]1C(OCC)=O.[ClH:15]>>[ClH:15].[ClH:15].[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][NH:2]1

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 18953633ethyl 1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxylate

생성물 1

HCID 189536441H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

실험 절차

10.4 g (51 mmol) of ethyl 2,3-dihydro-1H-pyrrolo-[3,4-c]pyridine-2-carboxylate are refluxed for 15 hours together with 100 ml of concentrated hydrochloric acid. The batch is evaporated, and the crystalline residue is stirred with acetone. The product is filtered off with suction and dried in the air.

후처리

  1. customThe batch is evaporated
  2. filtrationThe product is filtered off with suction
  3. customdried in the air

출처 및 근거

ORD 기록
ord-e690b9584d3b46ad8e37691ab0bf9ae7
출처 데이터셋
uspto-grants-1994_12
특허 번호
US05371090

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