Methyl iodide → HCID 178503988, 화합물

HRID 1492215노트

반응식

HRID 1492215 반응식
[CH3:1][C:2]1[C:7]([NH:8][C:9]([NH2:11])=[S:10])=[C:6]([N:12]2[CH2:17][CH2:16][O:15][CH2:14][CH2:13]2)[CH:5]=[CH:4][CH:3]=1.[CH3:18][I:19]>CC(C)=O>[IH:19].[CH3:18][S:10][C:9](=[NH:11])[NH:8][C:7]1[C:2]([CH3:1])=[CH:3][CH:4]=[CH:5][C:6]=1[N:12]1[CH2:17][CH2:16][O:15][CH2:14][CH2:13]1

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 15746509HCID 15746509, 화합물

생성물 1

HCID 178503988HCID 178503988, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of 1-(6-methyl-2-morpholinophenyl)thiourea (9 g) and methyl iodide (2.5 ml) in dry acetone (100 ml) was heated at reflux at 90°-95° C. for 2.5 hours to give 2-methyl-1-(6-methyl-2-morpholinophenyl)-2-thiopseudourea hydroiodide.

후처리

  1. temperaturewas heated
  2. temperatureat reflux at 90°-95° C. for 2.5 hours

출처 및 근거

ORD 기록
ord-3a014fe5e8b8473b97938e41076da994
출처 데이터셋
uspto-grants-1994_12
특허 번호
US05373008

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