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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1492759생성일: 2026년 10월 26일

2-Butyl-5-hydroxymethylimidazole → 2-Butyl-5-formylimidazole

https://huagongshe.com/reaction/1492759

반응식

참여 물질

역할이름HCID투입량
반응물2-Butyl-5-hydroxymethylimidazoleHCID 2735673—
촉매HCID 178418406HCID 178418406—
용매DichloromethaneHCID 6344—
용매1,4-DioxaneHCID 31275—
생성물2-Butyl-5-formylimidazoleHCID 273567184.8%

반응 단계

To a suspension of 2-butyl-1H-imidazole-5-methanol (2.02 g) in dry dichloromethane (40 ml) and dry dioxan (60 ml) was added manganese dioxide (7.05 g). The reaction mixture was heated at reflux for 3.5 h before being filtered, and the filtrate concentrated in vacuo to give the title compound as a white solid (1.69 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05374646
출처 데이터셋uspto-grants-1994_12
ORD IDord-6438c970a50e43988334c66cb57dc0f9
출처 메모uspto-grants-1994_12