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Lauryldimethylamine → Benzenemethanaminium, N-dodecyl-4-ethenyl-N,N-dimethyl-, chloride (1:1)

HRID 1496787
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인쇄 미리보기

반응식

HRID 1496787 반응식
[CH:1]([C:3]1[CH:10]=[CH:9][C:6]([CH2:7][Cl:8])=[CH:5][CH:4]=1)=[CH2:2].[CH3:11][N:12]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH3:13]>>[Cl-:8].[CH3:11][N+:12]([CH3:13])([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:7][C:6]1[CH:9]=[CH:10][C:3]([CH:1]=[CH2:2])=[CH:4][CH:5]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

3

반응물 2

HCID 8168LauryldimethylamineHCID 74126p-Vinylbenzyl chloride

생성물 1

HCID 6453318Benzenemethanaminium, N-dodecyl-4-ethenyl-N,N-dimethyl-, chloride (1:1)

실험 절차

Into a 200 ml flask were added 29.8 g of 4-vinylbenzyl chloride and 50 g of N,N-dimethyldodecylamine. The reaction mixture was stirred at room temperature for 24 h. The solid precipitate from the reaction was filtered, washed with diethyl ether, and dried under vacuum at room temperature.

후처리

  1. filtrationThe solid precipitate from the reaction was filtered
  2. washwashed with diethyl ether
  3. customdried under vacuum at room temperature

출처 및 근거

ORD 기록
ord-fbe17be959cd45d1827981ec595a85f8
출처 데이터셋
uspto-grants-2015_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09199203B2

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