Propanal → HCID 58500190, 화합물

HRID 1500170노트

반응식

HRID 1500170 반응식
[N+:1](/[CH:4]=[CH:5]/[CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1)([O-:3])=[O:2].[CH:12](=[O:15])[CH2:13][CH3:14].CC(O)C>CCCCCC>[CH:6]1([C@H:5]([CH2:4][N+:1]([O-:3])=[O:2])[C@H:13]([CH3:14])[CH:12]=[O:15])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1

참가 물질

5

반응물 3

HCID 527PropanalHCID 3776IsopropanolHCID 11094860132839-80-6

생성물 1

HCID 58500190HCID 58500190, 화합물

시약·촉매·용매 1

HCID 8058Hexane용매

실험 절차

The title compound was prepared from (E)-(2-nitrovinyl)cyclohexane and propionaldehyde according to general procedure. The enantiomeric excess was determined by HPLC with Chiralpak AD-H column at 210 nm (2-propanol:hexane=1:99), 1 mL/min, tmajor=17.0 min, tminor=19.1 min, the diastereomeric ratio was determined by

출처 및 근거

ORD 기록
ord-76c589482c8b41ef9d406608fb1e19ad
출처 데이터셋
uspto-grants-2015_12
특허 번호
US09206090B2

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