HCID 86644151, 화합물 → 2-Ethylpyridin-3-yl acetate
반응식
[C:1]([O:4][C:5]1[C:6]([C:11]#[CH:12])=[N:7][CH:8]=[CH:9][CH:10]=1)(=[O:3])[CH3:2]>C(O)C.O=[Pt]=O>[C:1]([O:4][C:5]1[C:6]([CH2:11][CH3:12])=[N:7][CH:8]=[CH:9][CH:10]=1)(=[O:3])[CH3:2]참가 물질
4
실험 절차
To a solution of 2-ethynylpyridin-3-yl acetate (5.0 g, 31 mmol) in ethanol (50 mL) was added PtO2 (0.50 g, 2.2 mmol). The mixture was degassed with nitrogen and placed under a double-layer balloon of hydrogen. The reaction was stirred at ambient temperature for 30 minutes. The mixture was filtered and concentrated in vacuo to give 2-ethylpyridin-3-yl acetate (5.1 g, 31 mmol) that was used without further purification.
후처리
- customThe mixture was degassed with nitrogen
- filtrationThe mixture was filtered
- concentrationconcentrated in vacuo
출처 및 근거
- ORD 기록
- ord-8cef54ad2ac24185b498ed074f201a19
- 출처 데이터셋
- uspto-grants-2012_07
- 특허 번호
- US08212045B2
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