HCID 87313423, 화합물 → HCID 87148504, 화합물

HRID 1511189노트

반응식

HRID 1511189 반응식
[C:1](=[N:5][C:6]1[C:11]([CH2:12][CH3:13])=[CH:10][C:9]([CH2:14][CH3:15])=[C:8]([N:16]=[C:17]([CH2:19][CH3:20])[CH3:18])[C:7]=1[CH3:21])([CH2:3][CH3:4])[CH3:2]>[Pt].CC(C)=O>[CH:17]([NH:16][C:8]1[C:9]([CH2:14][CH3:15])=[CH:10][C:11]([CH2:12][CH3:13])=[C:6]([NH:5][CH:1]([CH2:3][CH3:4])[CH3:2])[C:7]=1[CH3:21])([CH2:19][CH3:20])[CH3:18]

참가 물질

4

반응물 1

HCID 87313423HCID 87313423, 화합물

생성물 1

HCID 87148504HCID 87148504, 화합물

시약·촉매·용매 2

HCID 23939Platinum촉매HCID 180Acetone용매

실험 절차

N,N′-di-sec-butylidene-[diethyl(methyl)-1,3-benzenediamine] (28 g) and Pt(S)/C (2.8 g) were added to acetone (30 g) in an autoclave. The closed autoclave was purged 3 times with 125 psig (9.63×105 Pa) of H2 at 22° C. The mixture was kept at 21° C. and 125 psi (8.62×105 Pa) of H2 for 12 hours, forming the corresponding N,N′-di-sec-butyl-[diethyl(methyl)-1,3-benzenediamine] quantitatively.

후처리

  1. customThe closed autoclave was purged 3 times with 125 psig (9.63×105 Pa) of H2 at 22° C
  2. customwas kept at 21° C.

출처 및 근거

ORD 기록
ord-a066d47d375a43bea11eaf06cdd3ea23
출처 데이터셋
uspto-grants-2012_07
특허 번호
US08212078B2

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