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Ethyl formate → HCID 86639223, 화합물

HRID 1511614
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HRID 1511614 반응식
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][NH:7][CH2:8][CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11].[CH:15](OCC)=[O:16]>C1(C)C=CC=CC=1>[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][N:7]([CH:15]=[O:16])[CH2:8][CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 8025Ethyl formateHCID 14896429N-(2-Thienylmethyl)-β-alanine ethyl ester

생성물 1

HCID 86639223HCID 86639223, 화합물수율 99.9%

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Ethyl 3-[(thiophen-2-ylmethyl)amino]propionate (13.8 g) prepared in the step 1 and 47.8 g of ethyl formate were dissolved in 100 mL of toluene and heated to reflux overnight. After the reaction solution was cooled, the solvent was evaporated therefrom in vacuo to give 15.6 g of the objective compound as light yellow liquid.

후처리

  1. temperatureheated
  2. temperatureto reflux overnight
  3. temperatureAfter the reaction solution was cooled
  4. customthe solvent was evaporated

출처 및 근거

ORD 기록
ord-bc2babd608984d479558c4097b7a0a7d
출처 데이터셋
uspto-grants-2012_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08217031B2

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