Methyl iodide → HCID 68682905, 화합물

HRID 15201

반응식

HRID 15201 반응식
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[SH:8].[Cl:9][C:10]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:11]=1I.NC1C=CC(O)=CC=1Cl.CI>>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8][C:11]1[CH:12]=[CH:13][C:14]([O:16][CH3:17])=[CH:15][C:10]=1[Cl:9]

참가 물질

5

반응물 4

HCID 6328Methyl iodideHCID 805982-BromobenzenethiolHCID 871844-Amino-3-chlorophenolHCID 180015192-Chloro-1-iodo-4-methoxybenzene

생성물 1

HCID 68682905HCID 68682905, 화합물

실험 절차

Prepared from 2-bromo-benzenethiol and 2-chloro-1-iodo-4-methoxy-benzene (prepared from 4-amino-3-chloro-phenol by diazotization according to the general procedure by Tunney and Stille J. Org. Chem. 1987, 52, 748-753 followed by alkylation with methyl iodide according to the general procedure by Uozumi et al. J. Org. Chem. 1993, 58, 1945-1945)

출처 및 근거

ORD 기록
ord-df4420fb03d3464ea084d114a4475e52
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07732463B2

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