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Hydrochloric Acid → (3-Aminomethyl-5-chloro-4-fluoro-benzyl)-(2-methoxy-ethyl)-methyl-amine

HRID 1527497
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인쇄 미리보기

반응식

HRID 1527497 반응식
C(OC(=O)[NH:7][CH2:8][C:9]1[CH:14]=[C:13]([CH2:15][N:16]([CH2:18][CH2:19][O:20][CH3:21])[CH3:17])[CH:12]=[C:11]([Cl:22])[C:10]=1[F:23])(C)(C)C.Cl>O1CCOCC1>[NH2:7][CH2:8][C:9]1[CH:14]=[C:13]([CH:12]=[C:11]([Cl:22])[C:10]=1[F:23])[CH2:15][N:16]([CH2:18][CH2:19][O:20][CH3:21])[CH3:17]
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참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 68283786(3-Chloro-2-fluoro-5-{[(2-methoxy-ethyl)-methyl-amino]-methyl}-benzyl)-carbamic acid tert-butyl ester

생성물 1

HCID 68284515(3-Aminomethyl-5-chloro-4-fluoro-benzyl)-(2-methoxy-ethyl)-methyl-amine

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

was prepared according to Scheme C2 (step D) from (3-chloro-2-fluoro-5-{[(2-methoxy-ethyl)-methyl-amino]-methyl}-benzyl)-carbamic acid tert-butyl ester (222 mg, 0.47 mmol) and 4N HCl in dioxane. MS (LC-MS): 261.0 [M]+.

후처리

  1. customwas prepared

출처 및 근거

ORD 기록
ord-5028cc5dffa44f6b817a21bffc4b85d7
출처 데이터셋
uspto-grants-2015_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09085555B2

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