Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(3-(Dimethylamino)propyl)methacrylamide → 3-(Methacryloylamino)propyllauryldimethylammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(3-(Dimethylamino)propyl)methacrylamide | HCID 78882 | — |
| 반응물 | 1-Chlorododec-1-ene | HCID 122939 | — |
| 촉매 | Sulfuric Acid | HCID 1118 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 3-(Methacryloylamino)propyllauryldimethylammonium chloride | HCID 23064988 | — |
반응 단계
A mixture of 350 g of DMAPMA and 280 g of chlorododecene (1.5:1) was stirred with 111.2 g of water (15%) and 6 drops of concentrated sulfuric acid. The reaction mixture was heated up to 95°0 C. and N2 was bubbled through it. The conversion was followed by GC. After 24 hours the reaction mixture was cooled off (95% conversion of vinyl chloride) and product was further used in polymerization without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06207778B1 |
| 출처 데이터셋 | uspto-grants-2001_03 |
| ORD ID | ord-58644fbdba0343ebbc9a6f5cdf86b2ff |
| 출처 메모 | uspto-grants-2001_03 |